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<title>Memorandum from R. L. Murray and A. C. Menius to Dr. Clifford K.  Beck</title>
<title>[a machine-readable transcription]</title>
<author>Murray, Raymond L.</author>
<author>Menius, A. C.</author>
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<idno type="ETC"> Modern English, MurNBconcretefirst071451</idno>
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<p>Available from: NC State University Archives</p>
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<p n="public">URL: http://www.lib.ncsu.edu/archives/etext/engineering/reactor/murray/</p>
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<date>2000</date>
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<p>Nuclear Reactor Digitization Project</p>
<p>Raymond L. Murray Reactor Project Notebook</p>
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<title>Memorandum from R. L. Murray and A. C. Menius to Dr. Clifford K.  Beck</title>
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</editionStmt> <extent>2 pp.</extent>
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<idno>Manuscript copy consulted: NCSU Libraries call number UA105.16</idno>
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<text id="MurNBconcretefirst071451T">

<front><div1 type="summary" n="1">
<head><hi rend="bold"><hi rend="center">Memorandum from R. L. Murray and A. C. Menius to Dr. Clifford K.  Beck</hi><lb/>
<bibl><abbr>Typescript</abbr><lb/> <extent>2 pp.</extent> <lb/><date value="1951-07-14">July 14, 1951</date><lb/> <idno rend="suppress">MurNBconcretefirst071451</idno></bibl></hi></head>
<p>

</p>
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<body>
<pb n=""/>
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<figure entity="MurNBconcretefirst071451a"></figure></xref></seg></p>
<div1 type="memorandum" n="1">
<head><hi rend="italics">NCSC-25<lb/>July 14, 1951</hi></head>

<opener>TO:      <name type="person">Dr. Clifford K. Beck</name><lb/>
FROM:    <name type="person">R. L. Murray</name> and <name type="person">A. C. Menius</name><lb/>
SUBJECT: Reactor Concrete Tests (Preliminary Report)
</opener>
<p>This report summarizes the recent investigations of reactor concrete<lb/>
mixes by <name type="person">Professor C. R. Bramer</name> of the Civil Engineering Department. We are<lb/>
glad to report that the experiments were very successful, thanks to Mr. Bramer's<lb/>
ingenuity.</p>
<p>Two shipments of barytes aggregate were tested.<lb/>
<list><item>1.  <name type="place">Sweetwater, Tennessee</name> - supplied by <name type="person">L. A. Woods</name>.</item>
<item>2.  <name type="place">Cartersville, Georgia</name> - supplied by <name type="corporate">New Riverside Ochre Co.</name></item>
</list>
The first of these consisted of two separate sizes: what will be labeled<lb/>
"coarse," ranging from 1" maximum diameter stones to about 1/4", with very<lb/>
little fine material; what will be labeled "fine," ranging from a 1/4" maximum<lb/>
down below that transmitted by a 16 mesh screen; of the fine material 62&#x0025; goes<lb/>
through that screen, the rest is retained.<lb/>
<lb/>
The second shipment was a uniformly graded mixture ranging from 1" down to<lb/>
1/32".<lb/>
<lb/>
The Colemanite was the sand from the <name type="place">West Coast</name>; Portland cement types I, II<lb/>
and III (High-early) were on hand.
</p>
<p>In previous tests, the mortar had failed to set, which was attributed<lb/>
by <name type="place">Oak Ridge</name> people to be due to the large amount of water that is normally<lb/>
added to make the consistency proper for pouring. Thus in the present <orig reg="experiments">experi-<lb/>
ments</orig>, efforts were made to minimize the water content.<lb/>
<lb/>
As the basic proportions of materials, the <name type="place">Oak Ridge</name> Figures for a cubic yard<lb/>
were used:<lb/>
<list><item><table>
<row><cell>Barytes</cell><cell>3970 lb.</cell></row>
<row><cell>Colemanite</cell><cell>400 lb.</cell></row>
<row><cell>Portland Cement</cell><cell>830 lb.</cell></row>
<row><cell>Water</cell><cell>310 lb. (37.5 gal.)</cell></row>
</table>
</item></list></p>
<p>The following table gives the composition of the several batches used<lb/>
to make test cylinders:<lb/>
<list><head>A.  <date value="1951-06-19">June 19</date>:
</head>
<item>
One seventeenth (1/17) of the above weights were taken. Assuming that the<lb/>
Sweetwater barytes coarse was 3/4" ASTM and the fine was 3/8," the latter<lb/>
was <orig reg="screened">acreened</orig> to remove all material smaller than 16 mesh. The ratio of<lb/>
"coarse" to "new fine" was then taken as 16.6 to 1. The weights (in lb.)<lb/>
resulting were:</item>
<item><list><item>
<table>
<row><cell>Coarse barytes</cell><cell>220</cell><cell></cell></row>
<row><cell>New fine barytes</cell><cell>13.25</cell><cell>Air Temperature 80&#x00B0;</cell></row>
<row><cell>Colemanite</cell><cell>23.5</cell><cell>Humidity 70&#x0025;</cell></row>
<row><cell>Type III cement</cell><cell>48.8</cell><cell></cell></row>
</table></item></list>
</item></list></p>
<pb n='2'/>
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<p><list><item>One cylinder was made with 21.5 lb. of water which was 11.8&#x0025; more than the<lb/>
<name type="place">Oak Ridge</name> specification, the slump was negligible. A second was made with<lb/>
an arbitrary added amount of water giving a one-inch slump.</item>
<item>The first cylinder set up slowly, and after a week is still not completely<lb/>
firm; the second was even softer.</item></list></p>
<p>
<list><head>B. <date value="1951-06-21">June 21</date>.</head>
<item>The fraction of the cubic yard mix used in this case was 1/85. The <orig reg="alternative">alterna-<lb/>
tive</orig> of type II cement was tried, with the weights below:
</item>
<item>
<list><item>
<table>
<row><cell>Coarse barytes</cell><cell>44.05</cell><cell></cell></row>
<row><cell>New fine barytes</cell><cell>2.65</cell><cell>Air Temperature 82&#x00B0;</cell></row>
<row><cell>Colemanite</cell><cell>4.70</cell><cell>Humidity 76&#x0025;</cell></row>
<row><cell>Type II cement</cell><cell>9.80</cell><cell></cell></row>
<row><cell>Water</cell><cell>3.64 (Oak Ridge)</cell><cell></cell></row>
</table>
</item></list>
</item>
</list>
</p>
<p>
<list>
<head>C. <date value="1951-06-21">June 21</date>.</head>
<item>The fine barytes was not screened in this test. Proportions were adjusted<lb/>
somewhat:
</item>
<item>
<list><item>
<table>
<row><cell>Coarse barytes</cell><cell>36.05</cell><cell></cell></row>
<row><cell>Fine barytes</cell><cell>10.65</cell><cell>Temperature and Humidity as</cell></row>
<row><cell>Colemanite</cell><cell>4.70</cell><cell>above.</cell></row>
<row><cell>Type II cement</cell><cell>9.80</cell><cell></cell></row>
<row><cell>Water</cell><cell>4.14 (11.4&#x0025; over specification)</cell><cell></cell></row>
</table>
</item></list>
</item>
<item>Neither of these mixes have become firm or show any signs of even doing so.</item>
</list>
</p>
<p>
<list><head>D. <date value="1951-06-22">June 22</date>.</head>
<item>On the assumption that the dissolved colemanite inhibits the portland cement<lb/>
action, the colemenite was not added until the mixture of cement, aggregate<lb/>
and water had set for 45 minutes. The <name type="place">Georgia</name> barytes was used.
</item>
<item>
<list><item>
<table>
<row><cell>Barytes</cell><cell>46.70</cell><cell>Air temperature 82&#x00B0;</cell></row>
<row><cell>Colemanite</cell><cell>4.70</cell><cell>Humidity 75&#x0025;</cell></row>
<row><cell>Type III cement</cell><cell>9.80</cell><cell></cell></row>
<row><cell>Water</cell><cell>4.00 (11&#x0025; excess)</cell><cell></cell></row>
</table>
</item></list>
</item>
<item>This mix set up in about 24 hours and after three days is judged to be quite<lb/>
adequate.
</item>
</list></p>
<p>It would be concluded tentatively that:
<list>
<item>a.  <name type="place">Georgia</name> Barytes is a preferable aggregate, from the standpoint of<lb/>
uniformity of gradation (and cost).</item>
<item>b.  Type III cement should be used.</item>
<item>c.  Special "late" mixing of colemanite is needed.<lb/>
<name type="person">Professor Bramer</name> states that a contractor can do this.</item>
</list>

It is estimated that the water excess might be cut in half, or even more if a<lb/>
wetting agent such as Darex is used. Tests on those ideas and a neutron<lb/>
absorption experiment to determine whether the colemanite is uniformly enough<lb/>
distributed are planned.
</p>
<p>The specific gravity was measured to be 3.4.
</p>
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